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錄音名稱：	2045. Software Functions and Operation Procedure <上一個> <下一個>
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錄音文稿：	Click Start button in the left lower part of desktop and do as shown in figures below. Click “EDX3000” Click “Change/Remove” Click “OK”. Software Data Input & Backup Step 1: Click Start →All Programs →EDX 3000 and right click the shortcut icon in the menu on the right, select Properties in the dialog box appeared. Step 4: Find the folder data and copy it to another safe location. Note: If you want to restore original data, just need to recopy the backup to installation directory of the software. EDXRF3000 is precious metal analysis software developed by Skyray and the operation interface is as below. Ⅰ Software introduction 1 Menu bar It consists of Main, View, Curve, Spectrum, Report and Help. 1-1 Main 1) Normalize Device: assure the peak locations of tested elements are correct. 2) Setup Instrumental Parameter: a Voltage: control the high voltage values. b Current: control the current values of X-ray tubes. c Amplification(roughly): adjust the peak locations of elements roughly. d Amplification(fine): adjust the peak locations of elements finely. Note: When the value of amplification(roughly/fine) increases, peak locations of elements move rightwards; vice verse. e Do not adjust countrate: Select this button and the count rate of the material you test is just the countrate under the current X-ray tube’ Current . f Adjust countrate automatic: Select this button and the count rate is set as the value in the first textbox on the right according to the percentage in the second textbox while testing. 3) Preset measurement time: set measurement time for sample testing. 1-2 View 1) Hide ROI: display or hide boundary of element you selected in spectrum area. 2) Hide PKL: display or hide peak labels in spectrum area. 3) Hide Alynalysis Info: display or hide spectrum information in spectrum area. 1-3 Curve 1) New: build new working curves, enter curve names and click OK. 2) Open: open existing working curves. 3) Delete/rename: delete or modify existing working curves. 4) Interesting Elements: You can select elements to be tested by clicking them in the table below. 5) Set up ROI: select parts you are interested in from spectrum area. 6) Calculate Area of ROI: calculate areas of interested parts you have selected. 1-4 Spectrum 1) Save: save the spectra of samples tested. 2) Open: open the spectra saved. 3) Delete: delete the spectra saved. 4) qualitative analyse: display locations of elements in spectrum area. 5) qualitative analyse parameter: adjust the number of elements analyzed qualitatively in spectrum area. 6) Qualitative report: list elements analyzed qualitatively. 7) Calculate Intensity: use current spectrum for plotting working curve. Click Join Work Curve. 8) Reference Spectrum1/2: 1 adds a spectrum and 2 adds another one. 1-5 Report 1) Setup printer parameter: It sets relevant parameters of printer. 2) Print Spectrum: It prints current spectrum. 3) Report Content: It displays current testing results. 2 Tool bar Preset measurement time: set measurement times for different samples. Testing Organization Information Hide interested area: hide or display parts selected in spectrum area. Hide peak label: hide peak labels in spectrum area. Hide & Show Alynalysis Info New curve: build new working curves, input the curve name and click OK. Delete/rename curve: delete or modify existing working curves. Open curve: open existing working curves. Edit interested element: You can select elements to be tested by clicking them in the periodic table of elements. Edit content and intensity: edit contents and intensities of interested elements. Show work curve: display current working curves. Build peak label: build peak labels of elements. A peak label generally lies at the top of peak. Power scale: Click this item to build energy calibration after peak labels have been built. Save spectrum: save sample spectra you have obtained. Delete spectrum: delete sample spectra saved. Open spectrum: open sample spectra saved. Count intensity of the sample: use current spectrum for plotting working curve. Reference Spectrum&1: add a first reference spectrum. Reference Spectrum&2: add a second reference spectrum. Setup printer parameter: set corresponding parameters of the printer. Print spectrum line: print current spectrum. Inform content: display current testing results. Help: provide help files of the software. Exit 3 Others 1) Shortcut key area: There are six shortcut keys: Preset measurement time, Open curve, Open spectrum, Reference Spectrum&1, Inform content and Reference Spectrum&2. 2) The two buttons for controlling the testing are Start/Continue and Stop. 3) Parameter statuses of X-ray tube. 4) Current spectrum information. 5) Curve name, curve type and ready to calculate content or not. 6) Channel, energy and count rate of spectrum where current cross cursor lies. 7) Possible unknown elements and line series where cursor is when element is confirmed. 8) Interested elements for current working curve. 9) Fitted element of interested elements for current working curve. 10) Preset time for spectrum measurement and actual measurement time used. 11) General information of spectrum. 12) Spectrum area. Ⅱ Operation Procedure for Testing 1. Check if connection between the power cord and data cable are correct before you start the instrument. 2. The instrument should be preheated after you start it every day and preheat time is generally 30 minutes. Usually we take a Fe sample to preheat the instrument. 3. You can start testing after preheating. 1) Choose a corresponding curve according to the material you want to test. (eg: test gold material, you choose Au curve, test silver material, you choose Ag curve) 2) Open the reference spectrum of pure element that according to the curve you choose and lock it 3) Click Start to input the sample name and click OK. (when you test the material, you must make sure the spectrum of the material you test must be in the same position with the reference spectrum of the pure element) 4. Click Inform content to obtain the results after testing. 5. If you need to save the testing results to a directory, please select Save Report to File checkbox and click OK. Software Calibration Au curve Ⅰ. Establish working curve Click Curve →New, input curve name Au in dialog box appeared, and click OK. Click Curve →Open, select newly established curve Au in dialog box appeared, and click Open. Ⅱ. Edit Interested Elements Click Curve →Interesting Elements and Choose Interesting Elements dialog box appears. Select interested elements such as Fe, Co, Ni, Cu, Zn, Ru, Rh, Pd, Ag, Os, Ir, Pt, Au in Choose Interesting Elements dialog box. (The background of selected element is blue) Ⅲ. Set instrumental parameters and test pure samples and standard samples Set measurement time and instrumental parameters (see attachment), input pure element standard sample Fe, click Start, and input valid sample name Fe. Click OK and start to test, and click SpectrumSave to save the spectrum after testing. In a similar way, test other 7 pure elements including Ni, Cu, Zn, Pd(Pt14), Ag, Pt, Au and save the spectra. Click Reference Spectrum&1 in tool bar or SpectrumReference Spectrum&1 to open Au reference spectrum. Then test standard samples Au01, Au05, Au06, Au07, Au08, Au09, Au11, Au12, Au14, Au17, Au20, Au21, Au23 and Au24 and save the spectra. (Note: Keep La peaks of Au in these standard samples in the same position with those in reference spectra of Au while testing, and La and Lb peaks in standard samples shall not deviate from those in reference spectra, just see the interfaces as below) Ⅳ. Establish peak labels and energy calibration Open Cu reference spectrum, click Build peak label in tool bar or CurveSet up PKL, then right click at the top of Ka peak in Cu reference spectrum, a dialog box Build Peak Label appears and enter peak label name Cu. In a similar way, establish Ag peak label and click Power scale in tool bar or CurveEnergy Calibration. (Note: This step is very important, can not be ignored) Ⅴ. Choose intensity calculate methods and Establish element boundaries Interested elements selected before appear in interested element area of the interface. Select element Fe and right click, a hint box appears as below: Choose one calculate and fitting methods for each element(see attachment 2 ). Set Fe boundaries Open reference spectrum of Fe, the channel of lowest point on the left side of Ka peak is set as left boundary of Fe, and the channel of lowest point on the left side as its right boundary. Set boundaries of Ni, Cu and Zn First open Ni and Cu reference spectra The left boundary of Ni lies at its lowest point on the left side of Ka peak The right boundary of Ni lies at the cross point of Ka peaks of Ni and Cu Then open Cu and Zn reference spectra The left boundary of Cu is the channel of Ni’s right boundary +1 The right boundary of Cu lies at the cross point of Ka peaks of Cu and Zn The left boundary of Zn lies at the channel of the cross point of Ka peaks of Cu and Zn +1 The right boundary of Zn lies at the lowest point on the right side of its Ka peak Set Co boundaries The left boundary of Co is the channel of Fe’s right boundary +1 The right boundary of Co is the channel of Ni’s left boundary -1 The rule to set boundaries of Fe, Co, Ni, Cu and Zn: The boundaries of adjacent elements shouldn’t interference mutually Set boundaries of Ru, Rh, Pd and Ag Set boundaries of Ru and Rh: Mouse search technique(see attachment 4) is used to find peak channels of Ru and Rh, and left boundaries is the value of their peak channels -20, right boundaries is the value of their peak channels +20 Set Pd boundaries: Open Pd reference spectra, the left boundary of Pd lies at the lowest point on the left side of Ka peak, and right boundary at the lowest point on the right side Set Ag boundaries: Ag peak channel is in the middle of both boundaries, and both boundaries are 20 channels away from the peak channel. That is: its left boundary is the value of its peak channel(1105) -20, right boundary is the value of its peak channel(1105) +20. Set boundaries of Os, Ir, Pt and Au: Set boundaries of Os and Ir: Use mouse search technique to find peak channels of Os and Ir, left boundary of Os is the value of its peak channel -10, right boundary is the value of its peak channel +10; left boundary of Ir is the value of its peak channel -7, right boundary is the value of its peak channel +7 Set Pt boundaries: Open Pt reference spectrum, its left boundary lies at the cross point of crossing bar (60% in height of Lβ peak) and left part of Lβ peak; and its right boundary at the cross point of crossing bar (60% in height of Lβ peak) and right part of Lβ peak. (They are called secondary boundaries of Pt)(see attachment1) Set Au boundaries: Select primary boundaries of Au Ⅵ. Edit spectrum analysis information When boundaries of all interested elements are set, select any interested element and right click and select Show Spectrum Analyze, a dialog box appears as below. The calculation method of intensity is net area or gross area method. The fitted left boundary (RLeft) and right boundary (RRight) are -1 and do not need modification. The calculation method of intensity is multi-element spectrum fitting. And fitted left boundary (RLeft) and right boundary (RRight) of a element is its left boundary (PeakLeft) and right boundary (PeakRight). For example, both boundaries (PeakLeft & PeakRight) of Ni are 474 and 512, so the fitted boundaries (RLefe & RRight) of Ni are its both boundaries, namely 474 and 512. When we select intensity calculation method in step Ⅴ, we have edited relative effective elements of the elements whose calculation method of intensity is multi-element spectrum fitting. And the boundaries are fitted boundaries of relative effective elements. And the editing method is as below: We select the elements whose calculation method of intensity is multi-element spectrum fitting, and relevant information such as curve number, main element, fitted element, fitted left and right boundaries are displayed in CurveID, MainElement, FitElement, RLeft and RRight columns in Spectrum Analysis Information dialog box. Double click fitting boundaries area (RLeft or RRight) of relative elements in the second volume of the dialog box, as shown in figure below: A dialog box appears as below: Select OK. Find curve number (CurveID) in the third volume same as the one in the second volume of the dialog box, and enter boundaries of fitted elements in fitted boundaries area (RLeft or RRight). Click OK to exit after editing, then reopen Spectrum Analysis Information dialog box to confirm that all information in the second volume has been modified and exit. If not completely modified, need to reedit and confirm. For the element whose calculation method of intensity is pure element spectrum fitting, its fitted left (RLeft) and right (RRight) boundaries are left (PeakLeft) and right (PeakLeft) boundaries of it fitted pure element (namely main element). [Note: Pd, Ag and Au fit primary boundaries(see attachment 1) of Au, and Os, Ir and Pt fit secondary boundaries in Au curve.] Ⅶ. Calculate intensity According to characteristics of the curve to be established, open spectra of samples (Au01, Au05, Au06……) to be calculated and click Count intensity of the sample in tool bar or SpectrumCalculate Intensity in main menu. Then press Join Work Curve button. The samples for intensity calculation in Au curve are as following: Au01, Au05, Au06, Au07, Au08, Au09, Au11, Au12, Au14, Au17, Au20, Au21, Au23, Au24, Au-Fe, Au-Co, Au-Ni, Au-Zn, Au-Ru, Au-Rh, Au-Pd, Au-Os, Au-Ir and Au-Pt. Ⅷ. Edit content and intensity Input the contents of interested elements of standard samples in Edit Content and Intensity dialog box. If standard samples don’t contain some interested elements, input 0 in Content column. Edit contents and intensities of Au-Fe, Au-Co, Au-Ni, Au-Zn, Au-Ru, Au-Rh, Au-Pd, Au-Os, Au-Ir, Au-Pt samples The Cu content is 10.02 in standard sample Au11, and its intensity is known after calculation. According to the rule that adjacent elements in the same row have similar energies in periodic table of elements, set the content values as 10.02 for Fe, Co, Ni and Zn in Au-Fe, Au-Co, Au-Ni and Au-Zn samples, and calculate intensity values as following: Zn=1.2Cu, Ni=0.8Cu, Co=0.6Cu, Fe=0.6Cu. The Ag content is 10 in standard sample Au12, and its intensity is known after calculation. According to the rule that adjacent elements in the same row have similar energies in periodic table of elements, set the content and energy values of Ru, Rh and Pd in Au-Ru, Au-Rh and Au-Pd same as Ag content and intensity in Au12. In a similar way, the contents and intensities of Au-Os, Au-Ir are the same as those ones of Pt-Ir5% in Pt curve; the Pt content is 10 in Au-Pt, and intensity are twice of Ir intensity in Pt-Ir5% in Pt curve. Note: The rule applies to content editing of all interested elements: The higher content is, the higher intensity is. If any case violates that rule, double click the line where error exists to check the point (in red if checked) and disable it in establishing working curve. Ⅸ. Display and inspect working curve Click Show work curve in tool bar or CurveDisplay Work Curve in main menu, select Insert in Curve Type and Au in Element to be normalized. Choose any interested element in the Element column in the left part, and its working curve appears in the right part. (Note: The curves of all elements are in uptrend) If the parts between points are in downtrend in curve, as shown in figure below: Check if error occurs in selection in Edit Con & Inten, Curve Type and Element to be normalized; or error occurs in content and intensity editing or certain element has no content and intensity. Ⅹ. Test samples again and check the results Select some typical standard samples to test and check if the results are close to contents of standard samples. Calibration for other curves Pt curve 1 Curve name: Pt 2 Interested elements: Fe, Co, Ni, Cu, Zn, Ru, Rh, Pd, Ag, Os, Ir, Pt, Au, and intensity calculation methods of element contents are as follows: Net area: Fe, Co, Ru, Rh Multi-element fitting: Ni, Cu, Zn Correlative elements of Ni: Pt, Cu Correlative elements of Cu: Pt, Ni, Zn Correlative elements of Zn: Pt, Cu Pure element fitting: Pt, Pd, Ag, Os, Ir, Au, and Pt uses pure element fitting, Os, Ir and Au fit secondary boundaries of Pt, and Pd, Ag, Pt fit primary boundaries of Pt. 3 Test standard elements: Pt01, Pt03, Pt05, Pt07, Pt15, Pt-Ir5% 4 Establish boundaries: Pt boundaries are its primary boundaries, Au boundaries are secondary boundaries, and establishing other boundaries is similar to those in Au curve. 5 Establish spectrum analysis information: According to calculation method of element intensity and the steps are similar to those in Au curve. 6 Use Pt01, Pt03, Pt05, Pt07, Pt15, Pt-Fe, Pt-Co, Pt-Ni, Pt-Zn, Pt-Ru, Pt-Rh, Pt-Ag, Pt-Os and Pt-Au, and Pt-Ir5% to calculate and join to working curve 7 Edit content and intensity First input contents of known elements in the samples, for simulated samples Pt-Fe, Pt-Co, Pt-Ni, Pt-Zn, Pt-Ru, Pt-Rh, Pt-Ag, Pt-Os and Pt-Au, Pt content is 90 in Pt-Fe, Pt-Co, Pt-Ni and Pt-Zn, Pt intensity is equal to that in Pt15, the intensity relations between Fe, Co, Ni, Zn and Cu in Pt15 are as follows: Fe=Co=0.6Cu, Ni=0.8Cu, Zn=1.2Cu; Pt content is 89.8 in Pt-Ru, Pt-Rh and Pt-Ag, Pt intensity is equal to that in Pt05, the contents of Ru, Rh and Ag are 10.2 and the intensities are equal to Pd intensity in Pt05. In Pt-Au and Pt-Os, Au and Os content is both 5 and intensity of Au, Os is equal to Ir intensity in Pt-Ir5%, Pt content is 95 and Pt intensity is equal to that in Pt-Ir5%. 8 Display working curve: Select Insert in Curve Type and Pt in Element to be normalized. And others are same as those in Au curve. 9 Test samples again and check the results Pd curve 1 Curve name: Pd 2 Interested elements: Fe, Co, Ni, Cu, Zn, Ru, Rh, Pd, Ag, Os, Ir, Pt, Au, and calculation methods of element contents are as follows: Net area: Fe, Co, Ru, Rh Multi-element fitting: Ni, Cu, Zn, Pt, Au Correlative element of Ni: Pd, Cu Correlative element of Cu: Pd, Ni, Zn Correlative element of Zn: Pd, Cu Correlative element of Pt: Pd, Au Correlative element of Au: Pd, Pt Pure element fitting: Pd, Ag, Os, Ir, and Pd uses pure element fitting, fitted boundaries are same as Pd boundaries. 3 Test standard elements: Pd-Pt20% (Pt13), Pd-Cu10%, Pd-Ag10% 4 Establish boundaries: Similar to that in Au curve 5 Establish spectrum analysis information: According to calculation method of element intensity and the steps are similar to those in Au curve. 6 Use Pd-Pt20% (Pt13) , Pd-Cu10% and Pd-Ag10% to calculate working curve 7 Edit content and intensity First input contents of known elements in the samples, for simulated samples Pd-Fe, Pd-Co, Pd-Ni, Pd-Zn, Pd-Ru, Pd-Rh, Pd-Os, Pd-Ir and Pd-Au, Pt content is 10 in Pt-Fe, Pt-Co, Pt-Ni and Pt-Zn, Pt intensity is equal to that in Pt-Cu10%, the intensity relations between Fe, Co, Ni, Zn and Cu Pt-Cu10% are as follows: Fe=Co=0.6Cu, Ni=0.8Cu, Zn=1.2Cu; Pd content is 90 in Pd-Ru and Pd-Rh, Pd intensity is equal to that in Pd-Ag10%, the contents of Ru and Rh are 10 and the intensities are equal to Ag intensity in Pd-Ag10%. 8 Display working curve: Select Insert in Curve Type and Pd in Element to be normalized. And others are same as those in Au curve. 9 Test samples again and check the results Ag curve 1 Curve name: Ag 2 Interested elements: Ni, Cu, Zn, Ag Calculation methods of element contents are as follows: Multi-element fitting: Ni, Cu, Zn Correlative element of Ni: Ag, Cu Correlative element of Cu: Ag, Ni, Zn Correlative element of Zn: Ag, Cu Pure element fitting: Ag uses pure element fitting, and its fitted boundaries are its boundaries. 3 Test standard elements: Ag01, Ag05, Ag07, Ag08, Ag10, Ag11, Ag13 4 Establish boundaries: Similar to that in Au curve 5 Establish spectrum analysis information: According to calculation method of element intensity and the steps are similar to those in Au curve. 6 Use Ag01, Ag05, Ag07, Ag08, Ag10, Ag11 and Ag13 to calculate working curve 7 Edit content and intensity Input contents of known elements in the samples. 8 Display working curve: Select Insert in Curve Type and Ag in Element to be normalized. And others are same as those in Au curve. 9 Display working curve: Select Insert in Curve Type and Pd in Element to be normalized. And others are same as those in Au curve. That is all for calibration. Name of the product: Skyray X-ray Fluorescence Spectrometer Series and model number: Skyray Instrument EDX3000 Technical specifications Analysis range: 1ppm-99.99% Analytical range of elements: From sulfur to uranium Measuring object: powder, solid and liquid Measurement precision: 0.05% Measurement time: 60~300s Ambient temperature range: 15-30 Relative humidity: 70% Weight: 30kg Working voltage: AC 110/220V Configurations Single sample chamber Movable sample platform Si PIN semiconductor detector Amplifier circuit X-ray tube High and low voltage power supplies Detector: The measurement window of detector is made of beryllium membrane and fragile. It can be easily damaged by an external force. And the results of any operation on this window are regarded as man-made sabotage and Skyray is not responsible for it. 該錄音作品由錄音網原創制作并進行展示，未經許可不得盜用。更新日期：快來聽快來看，2014-5-4 11:04:00 錄音網新鮮出爐。Software Functions and Operation Procedure錄音，Software Functions and Operation Procedure錄音稿，Software Functions and Operation Procedure錄音文稿Software Functions and Operation Procedure配音，Software Functions and Operation Procedure配音稿，Software Functions and Operation Procedure配音文稿，Software Functions and Operation Procedure文稿錄制。關鍵字：課件,專題,企業錄音,課件,專題,企業配音,課件,專題,企業專業錄音,課件,專題,企業錄制。英語錄音,英語配音,英語專業錄音,英語錄制。男聲錄音,男聲配音,男聲專業錄音,男聲錄制。磁性,時尚錄音,磁性,時尚配音,磁性,時尚專業錄音,磁性,時尚錄制。錄音,配音,專業錄音,錄制。錄音,配音,專業錄音,錄制。錄音網,錄音網,錄音公司,廣告語錄音.
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