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1.we use in this manual the following caution marks as we refer to safety information or other crucial points. 2.You are suggested to read this chapter before using the instrument. 3.This does good to the operation of the instrument. 4.Jiangsu Skyray Instrument Co.,LTD.(hereafter Skyray) will warrant for free maintenance as long as they meet the following terms or premises: Product overview Introduction Product Name Skyray X-ray Fluorescence Spectrometer. Series and Model: Skyray Instrument EDX 6000B Features of the product: 1.Professional full-element analyzer of cement, steel and aggregate; also applicable to plating thickness measurement and RoHS testing 2.Vacuum sample chamber, good for analyzing light elements in low content 3.In-built SNE improves the signal processing ability up to 25 times. 4.The collimators and filters can be switched automatically for different samples. 5.Electric-cooling UHRD detector instead of liquid nitrogen cooling detector 6.Intelligent full-element analysis software matches with the hardware well. 7.Arbitrary optional analysis and identification models 8.Independent matrix effect correction models 9.Multi-variable non-linear regression procedure Technical specifications: 1.Measurable elements: Na to U 2.Range of element content: 1ppm-99.99% 3.Ability of simultaneous analysis: 24 elements 4.Detection limit: The detection limit of hazardous elements(Cd/Pb/Cr/Hg/Br)in RoHS directive reaches 1ppm. 5.Functions: RoHS, ores, plating thickness and full-element analysis; one instrument for multi purposes. 6.Plating thickness measurement: more than 11 layers, up to 0.005um each layer 7.Analysis accuracy: 0.05%(above 96%) 8.Forms of samples: powder, solid and liquid 9.Measurement time: 60s—200s 10.Ambient Temperature: 15℃—30℃ 11.Ambient Humidity: ≤70% 12.Working Voltage: AC 110V/220V Unique configurations: 1.Signal-to-Noise Enhancer (SNE) 2.Light path enhancement system 3.High efficient ultra thin end window X-ray tube 4.Electric-cooling UHRD detector 5.In-built high resolution CCD 6.Automatic collimator and filter switch 7.Enhanced metal sensitivity analyzer Unpacking and checking When you unpack the instrument, you would see the following articles: instrument, standard samples case, wall charts and accessory bag. Instrument、standard samples case、wall charts、accessory bag. Parts and functions Mainframe Movable sample chamber Telescopic supporting bar Buttons to lift and lower sample chamber cover HV indicator light Mains switch Auto turn plate Sample cup Mains switch USP port(to CCD) USP port(to PC) Fan (for heat dissipation) Power interface Fan (for heat dissipation) Vacuum interface Connecting the instrument 1.Connect one end of the power cord to the instrument and the other end to the socket. 2.Connect the pipe with the instrument 3.USB cable is used to control the CCD camera, one end of which connects to USB port on the instrument and the other end to USB port on PC. For safety reason, you are suggested not to touch the DOWN button when putting and taking the samples. For safety reason, you are suggested not to put any object within the scope of the movable sample chamber cover; otherwise, it may prevent the cover from closing. How to put the sample into the instrument for detection? 1.Press UP button till the sample chamber cover rises to the position you want it to. 2.Put the sample into the sample cup or on the ring. 3.Press DOWN button till the sample chamber cover closes. Then start the measurement. 4.Repeat the above steps to take the sample out after detection. I. Install the software Double click EDX6000B-XRF Setup.exe and enter the interface shown in Figure 1-1. Click “Next >” in Figure 1-1 and enter the interface shown in Figure 1-2. Click “Next >” in Figure 1-2 to enter the interface of Figure 1-3. Click “Change…” in Figure 1-3 and enter the interface shown in Figure 1-4. Click the button in the red marked zone and choose the installation directory of the software. After selecting the installation directory, click “OK” , see Figure 1-4. The interface then returns to Figure 1-3. Click “Next >” to enter Figure 1-5. Click “Install” in Figure 1-5 and then enter Figure 1-6. Click “Finish” in Figure 1-6 to complete the installation of the software. II. Running the software After the installation, double click “XRF.exe” on the desktop to run the software. See Figure 2-1. The main page of the software is shown as Figure 2-2. III. Calibrating the work curve 1. Parameter setting In figure 3-1, click “Parameter setting” and open the submenus “Interface” and “Content express”. Tick the corresponding options for them. 2. Set up work cure Click “WorkCurve” menu on the main page . See figure 3-2. Click the submenu “Open Work Curve” and then enter Figure 3-3. Click “Set up” in the red marked zone in Figure 3-3 and then enter Figure 3-4. Enter the name of the calibrating item in the box under “WorkCurve Name”, e.g. “stainless steel” and then click “Confirm” to complete the setup of the work curve. 3. Parameter setting Click “Initialization Parameter” from “WorkCurve ” on the main page, see Figure 3-5. Then set the parameters, see Figure 3-6. Click “Confirm” after all the parameters have been set. Click “Measurement Parameter” from “WorkCurve” on the main page, see Figure 3-7. Then set the parameters, see Figure 3-8. Click “Confirm” after all the parameters have been set. 4. Edit elements of interest Click “Edit Element” from “WorkCurve” on the main page, see Figure 3-9. In the prompt dialogue, select the elements of interest. Click “Confirm” after all elements of interest are selected. see Figure 3-10. 5.Scanning sample spectrum Initialization Before scanning the sample spectrum, initialize the instrument first. Place the Ag sample on the measurement platform and then click the initialization button in the red marked zone, see Figure 3-11. Click “OK” to start the initialization, see Figure 3-12. After the initialization, Figure 3-13 is displayed then. Scanning the sample spectrum Click “Start” in the red marketed zone in Figure 3-14 and then enter Figure 3-15. Figure 3-15 displays the “sample information” . Enter the name of the sample in the box after “Sample Name”. Select the testing times as required. Then tick the position of the sample in the “Chamber” column according to its actual location. Click “Confirm” to start scanning the spectrum, for instance: in the above figure, the sample is “Stainless steel 1#”, the measurement times is once and the sample position is 1#. Set the boundaries of the elements of interest Qualitative analysis Before setting the boundaries of the elements of interest, carry out the qualitative analysis first. The steps are as follows: Click the submenu “Display Peak Label” from “Qualitative Analysis”, see Figure 3-16. At this time, a column for setting up peak labels is displayed at the top of the spectrum area on the main page. See the red marked zone in Figure 3-17. Usually two peak labels are set up. Choose elements Cu and Ag. Select the submenu “Open” from “Working Spectrum”, see Figure 3-18. Then select “ag.Spe” and open it, see Figure 3-19. In the area of peak label setting, right mouse click to show the prompt menu and select “Add Peak Label”, see Figure 3-20. Then fill in the element Ag , select the characteristic X-rays Kа and click “Confirm”, see Figure 3-21. As shown in Figure 3-22 , Ag label has been set up. Use the same method to set up Cu label, see Figure 3-23. In Figure 3-24, select the submenu “Open” from “Working Spectrum” and then enter Figure 3-25. Select “stainless steel 1#” and open it. Select the submenu “Choose Qualitative Element” from “Qualitative analysis”, see Figure 3-26. Then select the elements of interest and their linear properties and click “Confirm”, see Figure 3-27. Select “Display Qualitative Element” from “Qualitative Analysis”, see Figure 3-28. At this time, in the spectrum area on the main page, the corresponding elements will be labeled, see Figure 3-29. Invoke the reference spectrum In Figure3-30, select the submenu “Reference Spectrum” from “Working Spectrum” and then enter Figure 3-31. Click “Set up” in Figure 3-31 enter Figure 3-32. Select “cr.Spe” and open it. In Figure 3-33, select “X Axis synchronization” and “Y Axis synchronization” in the red marked zone and click “Confirm”. At this time, the spectrum area on the main page will display the Cr reference spectrum. As shown in Figure 3-34, the red solid line is the spectrum. Set the boundaries On the tool bar, click “Zoom out” till the Cr peak can be clearly distinguished, see Figure 3-35. Select Cr element in the red marked zone in Figure 3-35. Right mouse click on the left side of Cr peak based on the reference spectrum and select “Peak Left”, see Figure 3-36, Then right mouse click on the right side of Cr peak based on the reference spectrum and select “Peak Right”, see Figure 3-37. To this point, the boundaries setting of Cr element is completed, shown as Figure 3-38. Boundaries setting of other elements of interest can be done in the same way. Intensity calculation In Figure 3-39, select the submenu “intensity method” from “WorkCurve” and then enter Figure 3-40. Select Mo in the red marked zone in Figure 3-40. Then tick the proper method from the 4 options under “Intensity Calculate Method”. If necessary, select the Peak/Background ratio, Peak Left and Peak Right. Or, if necessary, select the appropriate main element. If no main element exists, select the blank on the top of the list. Use this method to edit the calculation method of each element. After the setting, click “Save” and “Confirm”. Edit data In Figure 3-41, select the submenu “Edit data” from “WorkCurve” and then enter Figure 3-42. Click “Open” in Figure 3-42 and then enter Figure 3-43. Select the spectrum files involved in the calculation and open them. In Figure 3-44, enter the content of the elements corresponding to each sample in the “content” column marked by the red color. Then we get Figure 3-45. Click “Graph”(red) in Figure 3-45 to view the curve. Then we get Figure 3-46. Refer to the above-mentioned method, including editing the content of every element and checking the graph, to calibrate other work curves. Hereto, the calibration of work curve is completed. Ⅳ. Measuring unknown samples Initialization Before scanning the unknown sample, initialize the instrument first. Place the Ag sample on the measurement platform and click the initialization button in the red marked zone, see Figure 4-1. Then click “OK” when a hint pops up and start the initialization, see Figure 4-2. After the initialization, Figure 4-3 will be displayed. Scan the spectrum of the unknown sample Click “Start” in the red marked zone in Figure 4-4 and then enter Figure 4-5. Figure 4-5 displays the “sample Information”. Enter the name of sample in the box after “Sample Name”. Select the test times as required. And tick the position of the sample in “Chamber” (Red) column according to the actual location. Then click “Confirm” to start scanning the spectrum. As shown in Figure 4-6, the red zone displays the content of every element when the scanning of the unknown sample is completed. 該錄音作品由錄音網原創制作并進行展示,未經許可不得盜用。更新日期:快來聽快來看,2014-5-4 11:04:00 錄音網新鮮出爐。Product overview錄音,Product overview錄音稿,Product overview錄音文稿Product overview配音,Product overview配音稿,Product overview配音文稿,Product overview文稿錄制。 關鍵字:宣傳錄音,宣傳配音,宣傳專業錄音,宣傳錄制。英語錄音,英語配音,英語專業錄音,英語錄制。男聲錄音,男聲配音,男聲專業錄音,男聲錄制。渾厚,穩重,成熟錄音,渾厚,穩重,成熟配音,渾厚,穩重,成熟專業錄音,渾厚,穩重,成熟錄制。錄音,配音,專業錄音,錄制。錄音,配音,專業錄音,錄制。錄音網,錄音網,錄音公司,廣告語錄音.
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